Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Benzoic acid, 2-(aminosulfonyl)-, methyl ester
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Saccharin | HCID 5143 | — |
| 생성물 | Benzoic acid, 2-(aminosulfonyl)-, methyl ester | HCID 42546 | — |
반응 단계
An HCl stream is led under cooling into a suspension of 143.3 g (0.78 mol) in 600 ml absolute methanol until saturation. Subsequently the solution is refluxed yet two hours until the saccharine has gone completely into solution and the reaction has terminated.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04601746 |
| 출처 데이터셋 | uspto-grants-1986_07 |
| ORD ID | ord-7682b66929384626b8eedbdba4fb52da |
| 출처 메모 | uspto-grants-1986_07 |