HCID 13656160, 화합물 → HCID 13656162, 화합물

HRID 745908노트

반응식

HRID 745908 반응식
C(OC([NH:11][CH2:12][CH:13]([OH:40])[CH2:14][CH2:15][CH:16]([NH:27][CH:28]([C:37]([OH:39])=[O:38])[CH2:29][CH2:30][C:31]1[CH:36]=[CH:35][CH:34]=[CH:33][CH:32]=1)[C:17]([N:19]1[CH2:26][CH2:25][CH2:24][C@H:20]1[C:21]([OH:23])=[O:22])=[O:18])=O)C1C=CC=CC=1>C(O)C.[Pd]>[NH2:11][CH2:12][CH:13]([OH:40])[CH2:14][CH2:15][CH:16]([NH:27][CH:28]([C:37]([OH:39])=[O:38])[CH2:29][CH2:30][C:31]1[CH:32]=[CH:33][CH:34]=[CH:35][CH:36]=1)[C:17]([N:19]1[CH2:26][CH2:25][CH2:24][C@H:20]1[C:21]([OH:23])=[O:22])=[O:18]

참가 물질

4

반응물 1

HCID 13656160HCID 13656160, 화합물

생성물 1

HCID 13656162HCID 13656162, 화합물

시약·촉매·용매 2

HCID 23938Palladium촉매HCID 702Ethanol용매

실험 절차

Compound VII in ethanol was hydrogenated at 40 psi at room temperature for 24 hours using 10% Pd/C. Filtration, purification over LH-20 and freeze drying gave VIII.

후처리

  1. filtrationFiltration, purification over LH-20
  2. customfreeze drying

출처 및 근거

ORD 기록
ord-237f8868d3594245b728a7c689803a9f
출처 데이터셋
uspto-grants-1986_07
특허 번호
US04602002

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