Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
tert-Butyl carbazate → tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | tert-Butyl carbazate | HCID 70091 | — |
| 반응물 | 2-Quinolinecarboxaldehyde | HCID 79619 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | tert-butyl N'-(quinolin-2-yl)methylene-hydrazinecarboxylate | HCID 69201455 | — |
반응 단계
A solution of 10.70 g 2-quinolinecarboxaldehyde and 9.00 g tert-butyl hydrazinecarboxylate in 200 ml of ethanol is refluxed for 2 h with stirring. Then the solution is evaporated to dryness and the residue is triturated with diisopropylether, separated off and dried at 50° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07393847B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-b0c24742b0534cffba3d932cbf487f85 |
| 출처 메모 | uspto-grants-2008_07 |