Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Cadaverine → N-(5-Aminopentyl)benzamide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Cadaverine | HCID 273 | — |
| 반응물 | Benzamide | HCID 2331 | — |
| 생성물 | N-(5-Aminopentyl)benzamide | HCID 345353 | 70.6% |
반응 단계
Under an argon atmosphere, 1,5-diaminopentane (25 g, 0.24 mol) and benzamide (9.9 g, 0.081 mol) were combined and heated at reflux overnight. The reaction mixture was concentrated under vacuum to remove the excess diamine. The residue was distilled at about 210° C. at 12 torr (16×102 pascals) to provide 11.8 g of N-(5-aminopentyl)benzamide as a colorless oil.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07393859B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-6b93c46bf3af424ba9e6805efc66fcec |
| 출처 메모 | uspto-grants-2008_07 |