Potassium Iodide → HCID 69299641, 화합물
반응식
[F:1][C:2]1[CH:3]=[C:4]([C:10]2[CH:15]=[CH:14][C:13]([OH:16])=[CH:12][CH:11]=2)[CH:5]=[CH:6][C:7]=1[C:8]#[N:9].Br[CH2:18][CH2:19][O:20][CH3:21].[I-].[K+].C(=O)([O-])[O-].[K+].[K+]>CC(=O)CC>[F:1][C:2]1[CH:3]=[C:4]([C:10]2[CH:15]=[CH:14][C:13]([O:16][CH2:18][CH2:19][O:20][CH3:21])=[CH:12][CH:11]=2)[CH:5]=[CH:6][C:7]=1[C:8]#[N:9]참가 물질
6
실험 절차
A mixture of 3-fluoro-4′-hydroxy-1,1′-biphenyl-4-carbonitrile (0.50 g, 2.35×10−3 mol), 1-bromo-2-methoxyethane (0.33 g, 2.35×10−3 mol), potassium iodide (0.04 g, 2.35×10−4 mol) and potassium carbonate (1.30 g, 9.40×10−3 mol) in butanone (20 cm3) was reacted, worked up and purified as described for compound 3 in Example 2. Yield 0.40 g (63%), GC purity (99.86%).
후처리
- customwas reacted
- custompurified
출처 및 근거
- ORD 기록
- ord-e40f0fd3fe574bbbbf7bf2ba072ebddc
- 출처 데이터셋
- uspto-grants-2008_07
- 특허 번호
- US07396487B2
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