Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
n,n-Bis(2-cyanoethyl)hexylamine → n,n-Bis(3-aminopropyl)hexylamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | n,n-Bis(2-cyanoethyl)hexylamine | HCID 16733110 | — |
| 반응물 | HCID 178418361 | HCID 178418361 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | n,n-Bis(3-aminopropyl)hexylamine | HCID 16733236 | 100.6% |
반응 단계
31.0 g of N,N-bis(2-cyanoethyl)hexylamine, 4.65 g of RaneyCo, 150 ml of 1,4-dioxane was charged to an autoclave, and hydrogen addition reaction was carried out by supplying hydrogen at an initial pressure of 9.1 MPa at 110° C. for 2 hours. After removing a catalyst by filtration, the obtained filtrate was concentrated and dried to obtain 32.4 g of a target compound as a pale red oily product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08830811B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-7e8ee36758c7485db6b2a8f14bebde0b |
| 출처 메모 | uspto-grants-2014_09 |