N,N-Dimethyl-1,3-propanediamine → HCID 22350930, 화합물

HRID 747534노트

반응식

HRID 747534 반응식
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[NH:7][C:8](=[S:12])SCC.[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH2:18]>C(O)C>[CH3:13][N:14]([CH3:19])[CH2:15][CH2:16][CH2:17][NH:18][C:8]([NH:7][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][N:1]=1)=[S:12]

참가 물질

4

반응물 2

HCID 7993N,N-Dimethyl-1,3-propanediamineHCID 12214896Ethyl 2-Pyridyldithiocarbamate

생성물 1

HCID 22350930HCID 22350930, 화합물

시약·촉매·용매 1

HCID 702Ethanol용매

실험 절차

A mixture of ethyl 2-pyridyldithiocarbamate (600 mg), 3-(dimethylamino)propylamine (0.38 ml) and ethanol (6 ml) was heated with reflux under nitrogen atmosphere. One and half hour thereafter, the reaction mixture was concentrated under reduced pressure to give the title compound (786 mg) as crude oil.

후처리

  1. temperaturewas heated
  2. temperaturewith reflux under nitrogen atmosphere
  3. concentrationOne and half hour thereafter, the reaction mixture was concentrated under reduced pressure

출처 및 근거

ORD 기록
ord-c55300dbfc144f439c6f699b2f6b1245
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07396842B2

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