Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Ethyl 4-cyanobenzoate | HCID 81589 | — |
| 용매 | 1,4-Dioxane | HCID 31275 | — |
| 생성물 | Ethyl 4-ethoxycarbonimidoylbenzoate hydrochloride | HCID 68830640 | — |
반응 단계
5.16 g (29 mmol) of ethyl 4-cyanobenzoate was stirred in 50 ml of 4N solution of hydrogen chloride in dioxane. 5 ml of ethanol was added to the resultant mixture, and they were stirred at room temperature for 4 days. The solvent was evaporated, and the residue was washed with ethyl acetate and dried to obtain the title compound.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07396844B1 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-745c474fe6424adb93f48ea986009b47 |
| 출처 메모 | uspto-grants-2008_07 |