Ethanol → Ethyl sulfoacetate

HRID 747777

반응식

[S:1]([CH2:5][C:6]([OH:8])=[O:7])([OH:4])(=[O:3])=[O:2].[CH2:9](O)[CH3:10]>>[S:1]([CH2:5][C:6]([O:8][CH2:9][CH3:10])=[O:7])([OH:4])(=[O:3])=[O:2]

참가 물질

반응물 2

HCID 702Ethanol

HCID 31257Sulfoacetic acid

생성물 1

HCID 12216623Ethyl sulfoacetate

반응 조건

온도: 80 °C

실험 절차

2.21 g (15.8 mmol) of sulfoacetic acid was suspended in 30 ml of ethanol, and the suspension was heated at 80° C. under reflux for 5 hours. The solvent was distilled off to obtain the title compound.

후처리

temperatureunder reflux for 5 hours
distillationThe solvent was distilled off

출처 및 근거

ORD 기록: ord-7c0ee0c177f14bd0af3e41d8c0c28fe5
출처 데이터셋: uspto-grants-2008_07
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US07396844B1

연결된 노트

불러오는 중…