Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Bis(2-ethylhexyl) phosphate → Potassium bis(2-ethylhexyl) phosphate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Bis(2-ethylhexyl) phosphate | HCID 9275 | — |
| 반응물 | Potassium Hydroxide | HCID 14797 | — |
| 반응물 | Potassium hydride | HCID 82127 | — |
| 반응물 | Potassium | HCID 5462222 | — |
| 용매 | Heptane | HCID 8900 | — |
| 생성물 | Potassium bis(2-ethylhexyl) phosphate | HCID 23675922 | — |
반응 단계
The potassium salt of bis(2-ethylhexyl) hydrogen phosphate was made by the direct reaction of potassium hydride with the corresponding acid in heptane. The acid bis(2-ethylhexyl) hydrogen phosphate (Aldrich Chemicals; 64.49 grams or 0.2 moles) was placed in 300 ml of dry heptane and stirred gently. An excess of potassium hydroxide granules was added to the solution and left to stir until no further potassium hydroxide reacted. At completion the reaction solution was decanted and the heptane evaporated to leave the potassium bis(2-ethylhexyl) phosphate salt as a white waxy solid.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07399731B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-b4bd8634624845dba2efd597a5be4759 |
| 출처 메모 | uspto-grants-2008_07 |