Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-(Phenylmethyl)propanedinitrile → 2-Benzyl-2-(3,4,4-trifluoro-3-butenyl)malononitrile
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-(Phenylmethyl)propanedinitrile | HCID 15846 | — |
| 반응물 | Sodium hydride | HCID 24758 | — |
| 반응물 | 4-Bromo-1,1,2-trifluorobut-1-ene | HCID 66333 | — |
| 용매 | Dimethylformamide | HCID 6228 | — |
| 생성물 | 2-Benzyl-2-(3,4,4-trifluoro-3-butenyl)malononitrile | HCID 22234999 | 75.1% |
반응 단계
Using 0.1 g of benzylmalononitrile, 5 ml of N,N-dimethylformamide, 0.010 g of sodium hydride (60% in oil), and 0.04 g of 4-bromo-1,1,2-trifluoro-1-butene, and according to the process described in the Production Example 1, there was obtained 0.042 g of 2-benzyl-2-(3,4,4-trifluoro-3-butenyl)malononitrile (the present compound (4)).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07402691B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-cda3e338e4a246658101ae94a38aba97 |
| 출처 메모 | uspto-grants-2008_07 |