Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Tetramethyl cyclobutane-1,2,3,4-tetracarboxylatato(2-) → 1,2,3,4-Cyclobutanetetracarboxylic Acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Tetramethyl cyclobutane-1,2,3,4-tetracarboxylatato(2-) | HCID 266035 | — |
| 용매 | Hydrochloric Acid | HCID 313 | — |
| 생성물 | 1,2,3,4-Cyclobutanetetracarboxylic Acid | HCID 266034 | 88.2% |
반응 단계
The resultant tetramethyl cyclobutane-1,2,3,4-tetracarboxylate (1224 g, 4.25 mol) and aqueous hydrochloric acid (3000 ml) were added to a 5-liter flask; reacted at a controlled temperature of 85° C. for 24 hours; cooled to room temperature; concentrated; and dried to obtain cyclobutane-1,2,3,4-tetracarboxylic acid (870 g, 3.75 mol).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07402693B2 |
| 출처 데이터셋 | uspto-grants-2008_07 |
| ORD ID | ord-fc15c68955324ce5a28bd88a6b93d097 |
| 출처 메모 | uspto-grants-2008_07 |