Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2-Bromo-2-methylpropionyl bromide → 11-Mercaptoundecyl 2-Bromo-2-methylpropanoate
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2-Bromo-2-methylpropionyl bromide | HCID 88685 | — |
| 반응물 | 11-Mercaptoundecanol | HCID 261824 | — |
| 생성물 | 11-Mercaptoundecyl 2-Bromo-2-methylpropanoate | HCID 57539288 | — |
반응 단계
Mercaptoundecyl bromoisobutyrate was synthesized through the reaction of bromoisobutyryl bromide and 11-mercapto-1-undecanol using a method published previously. 1H NMR (300 MHz, CDCl3): 4.15 (t, J=6.9 Hz, 2H, OCH2), 2.51 (q, J=7.5 Hz, 2H, SCH2), 1.92 (s, 6H, CH3), 1.57-1.72 (m, 4H, CH2), and 1.24-1.40 (m, 16H, CH2).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835144B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-acb88dfe21004e37bae13606ba9b6b2c |
| 출처 메모 | uspto-grants-2014_09 |