5-Amino-2,2-dimethyl-2H-chromene-8-carbonitrile → 2-(Allyloxy)-4-aminobenzonitrile

HRID 751051

반응식

HRID 751051 반응식
[CH2:1]([O:4][C:5]1[CH:12]=[C:11]([N+:13]([O-])=O)[CH:10]=[CH:9][C:6]=1[C:7]#[N:8])[CH:2]=[CH2:3].NC1C=CC(C#N)=C2C=1C=CC(C)(C)O2>>[CH2:1]([O:4][C:5]1[CH:12]=[C:11]([NH2:13])[CH:10]=[CH:9][C:6]=1[C:7]#[N:8])[CH:2]=[CH2:3]

참가 물질

3

반응물 2

HCID 597542965-Amino-2,2-dimethyl-2H-chromene-8-carbonitrileHCID 597543072-(Allyloxy)-4-nitrobenzonitrile

생성물 1

HCID 597542362-(Allyloxy)-4-aminobenzonitrile수율 97.6%

실험 절차

The title compound (1.70 g) as a light yellow solid was prepared from compound 10A (2.04 g, 10 mmol) by procedures analogous to those described in Experiment 6C.

출처 및 근거

ORD 기록
ord-fa812366a55c465e93f387a9d0715b6d
출처 데이터셋
uspto-grants-2008_07
특허 번호
US07405234B2

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