Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
4-Hydroxybenzoic Acid → Benzoic acid, 4-((1-oxodecyl)oxy)-
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 4-Hydroxybenzoic Acid | HCID 135 | — |
| 반응물 | Pyridine | HCID 1049 | — |
| 반응물 | Decanoyl chloride | HCID 66982 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Benzoic acid, 4-((1-oxodecyl)oxy)- | HCID 3608562 | — |
반응 단계
10 Grams of p-hydroxybenzoic acid and 15 g of decanoic acid chloride were stirred at room temperature, and 7.2 g of pyridine was dropwise added. After the mixture was stirred for 1 day, a reaction product was poured into water, and an organic layer was extracted with dichloromethane. The organic layer was washed with 1N hydrochloric acid and dried over anhydrous sodium sulfate, the solvent was distilled off, and then residue was washed with n-hexane and then dried to give a crude end product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US05723069 |
| 출처 데이터셋 | uspto-grants-1998_03 |
| ORD ID | ord-c218088b16c541088a933a7606f68c4c |
| 출처 메모 | uspto-grants-1998_03 |