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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 7525생성일: 2026년 10월 23일

Acetyl chloride → HCID 178419033, 화합물

https://huagongshe.com/ko/reaction/7525

반응식

참여 물질

역할이름HCID투입량
반응물Acetyl chlorideHCID 6367—
반응물2-AminopyrimidineHCID 7978—
반응물2-PyridinecarboxaldehydeHCID 14273—
반응물Cyclohexyl isocyanideHCID 79129—
용매Perchloric AcidHCID 24247—
생성물HCID 178419033HCID 178419033—

반응 단계

Example 19 was carried out in accordance with the general directions for synthesis in process step a) from 1.0 ml (0.1 mmol) 2-amino-pyrimidine (0.1 M, DCM), 0.575 ml (0.115 mmol) cyclohexylisonitrile solution (0.2 M, DCM), 0.500 ml (0.15 mmol) pyridine-2-carbaldehyde solution (0.3 M, DCM) and 10 μl perchloric acid (w=20%) and in process step c) and d) by reacting the resultant reaction product with 0.4 mmol acetylchloride.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US07087607B2
출처 데이터셋uspto-grants-2006_08
ORD IDord-1cc3531c804049d985d00a34b502b64b
출처 메모uspto-grants-2006_08