참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Phenyl Isothiocyanate | HCID 7673 | — |
| 반응물 | 4,4'-Diaminobenzanilide | HCID 69917 | — |
| 용매 | Acetone | HCID 180 | — |
| 생성물 | 4,4'-Di(phenylthiocarbamoylamino)benzanilide | HCID 19693281 | 72.3% |
반응 단계
4,4'-Diaminobenzanilide (0.658 g, 2.5 mM) was dissolved in 20 ml of acetone, and 2 equivalents of phenylisothiocyanate (0.676 g, 5 mM) was added. The mixture was stirred at 55° C. for 10 minutes. After cooling, the reaction mixture was filtered, and washed with acetone/n-hexane to obtain 0.90 g (72.3% yield) of a colorless crystal of compound A-15.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723075 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-e8642ae0ecb248809067cd131fde0eed |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
