Cyclopentanecarbonyl chloride → N-{1-[3-(3-Nitrophenyl)-5-oxo-4,5-dihydro-1,2,4-triazin-6-yl]propyl}cyclopentanecarboxamide
반응식
[NH2:1][CH:2]([C:5]1[C:6](=[O:20])[NH:7][C:8]([C:11]2[CH:16]=[CH:15][CH:14]=[C:13]([N+:17]([O-:19])=[O:18])[CH:12]=2)=[N:9][N:10]=1)[CH2:3][CH3:4].[CH:21]1([C:26](Cl)=[O:27])[CH2:25][CH2:24][CH2:23][CH2:22]1>>[N+:17]([C:13]1[CH:12]=[C:11]([C:8]2[NH:7][C:6](=[O:20])[C:5]([CH:2]([NH:1][C:26]([CH:21]3[CH2:25][CH2:24][CH2:23][CH2:22]3)=[O:27])[CH2:3][CH3:4])=[N:10][N:9]=2)[CH:16]=[CH:15][CH:14]=1)([O-:19])=[O:18]참가 물질
3
실험 절차
In analogy to the procedure for Example 36A, 3.0 g (10.9 mmol) 6-(1-aminopropyl)-3-(3-nitrophenyl)-1,2,4-triazin-5(4H)-one, 2.2 g (16.3 mmol) cyclopentanecarbonyl chloride and proportionate amounts of the other reagents are used.
출처 및 근거
- ORD 기록
- ord-fea17c083a1e486d9dd4e00e7e5ed49c
- 출처 데이터셋
- uspto-grants-2006_08