2-Phenylisobutyric acid → HCID 178492372, 화합물

반응식

COc1ccc(N)cc1C.CC(C)(C(=O)O)c1ccccc1.C1CCN(C1)C(=[N+]2CCCC2)ON3C4=CC=CC=C4N=N3.F[P-](F)(F)(F)(F)F.CN(C)C=O>>COc1ccc(NC(=O)C(C)(C)c2ccccc2)cc1C

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

불러오는 중…

addition150 uL of MeCN/H2O (1:1) mixed solvent was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
addition150 uL of internal standard solution was dispensed separately into each plate using the 96-tip head of the Tecan Evo-200.
aliquot10 uL aliquot taken from reaction vials, and added to pre-filled wells in the transfer plate.
addition380 uL MeCN solvent were added to the transfer plate
aliquot20 uL taken from transfer plate to filter plate 1 for LCMS analysis
addition180 uL MeCN added to filter plate 1 for LCMS analysis
aliquot10 uL taken from transfer plate to filter plate 2 for TOF-DESI analysis
addition190 uL MeCN added to filter plate 2 for TOF-DESI analysis
customthe 96-well filter plates were centrifuged for 2.5 min at 3000 RPM

불러오는 중…