참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzyl Isothiocyanate | HCID 2346 | — |
| 반응물 | P-Phenylenediamine | HCID 7814 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 1,4-Di(benzylthiocarbamoylamino)benzene | HCID 19693305 | 61.6% |
반응 단계
p-Phenylenediamine (2.707 g, 25 mM) was dissolved in 20 ml of ethyl acetate, and 2 equivalents of benzylisothiocyanate (7.461 g, 50 mM) were added. The mixture was stirred at 80° C. for 30 minutes. After cooling, the reaction mixture was filtered, and washed with ethylacetate/n-hexane to obtain 6.26 g (61.6% yield) of a colorless crystal of compound A-25.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723075 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-96af32b871984951b1483d8522037b06 |
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| 출처 메모 | uspto-grants-1998_03 |
|---|
