Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Nitric Acid → 4-(Benzyloxy)-5-methoxy-2-nitrobenzaldehyde
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Nitric Acid | HCID 944 | — |
| 반응물 | 4-(Benzyloxy)-3-methoxybenzaldehyde | HCID 75506 | — |
| 생성물 | 4-(Benzyloxy)-5-methoxy-2-nitrobenzaldehyde | HCID 561363 | 87% |
반응 단계
Nitric acid (100 mL) was cooled to 0° C., 4-benzyloxy-3-methoxybenzaldehyde (20 g, 82.55 mmol) was added dropwise, and the mixture was stirred at room temperature for 2 hours. After completion of the reaction, distilled water was added thereto and the mixture was stirred for 30 min, followed by filtration of the solid to obtain the title compound (20.52 g, 87%).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835458B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-829124fe01be4f0d845d1c70aca583ab |
| 출처 메모 | uspto-grants-2014_09 |