Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Potassium Bromide → 3-[4-(3-Cyclohexyl-ureido)-phenyl]-isoxazole-5-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Potassium Bromide | HCID 253877 | — |
| 반응물 | HCID 67354653 | HCID 67354653 | — |
| 생성물 | 3-[4-(3-Cyclohexyl-ureido)-phenyl]-isoxazole-5-carboxylic acid | HCID 67352849 | 92% |
반응 단계
The title compound was prepared from 3-[4-(3-cyclohexyl-ureido)-phenyl]-isoxazole-5-carboxylic acid ethyl ester as set forth in Example 8 and was obtained in 92% yield. Mass (ES+): 330 (M++1); IR (KBr): 3318, 2927, 2853, 1711, 1637, 1563; 1H NMR (DMSO-d6) δ: 1.05-1.80 (4×m, 10H), 3.45 (br, 1H), 6.17 (d, 1H), 7.49 (d, 2H), 7.66 (s, 1H), 7.79 (d, 2H), 8.58 (s, 1H), 14.5 (br, ˜0.5H).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835428B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-4dacd620a29e4a369674d3405a3a8192 |
| 출처 메모 | uspto-grants-2014_09 |