참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Benzyl Isothiocyanate | HCID 2346 | — |
| 반응물 | 1,5-Diaminonaphthalene | HCID 16720 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | 1,5-Di(benzylthiocarbamoylamino)naphthalene | HCID 19693280 | 30.7% |
반응 단계
1,5-Naphthalenediamine (0.791 g, 5 mM) was dissolved in 20 ml of ethyl acetate, and 2 equivalents of benzylisothiocyanate (1.492 g, 10 mM) were added. The mixture was stirred at 80° C. for 30 minutes. After cooling, the reaction mixture was filtered, and washed with ethylacetate/n-hexane to obtain 0.70 g (30.7% yield) of a colorless crystal of compound A-29.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US05723075 |
|---|
| 출처 데이터셋 | uspto-grants-1998_03 |
|---|
| ORD ID | ord-d421bcbbd72f4cb18c2bcf8464545117 |
|---|
| 출처 메모 | uspto-grants-1998_03 |
|---|
