Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
1,2-Ethanediamine, N1,N1,N2-trimethyl- → Bis-benzyloxy benzoic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 1,2-Ethanediamine, N1,N1,N2-trimethyl- | HCID 67338 | — |
| 반응물 | Methyl 2,3-bis(benzyloxy)benzoate | HCID 10665397 | — |
| 생성물 | Bis-benzyloxy benzoic acid | HCID 10520703 | — |
반응 단계
In another embodiment the compounds can be prepared as shown in Scheme IV. A bromo-nitrobenzene (1) can be reacted with N1,N2,N2-trimethylethane-1,2-diamine to give N1-(nitrophenyl)-N1,N2, N2-trimethylethane-1,2-diamine (2). A solution of (2) in can be subjected to hydrogenation, passed through a short pad of celite, washed with MeOH and evaporated under reduced pressure. Thiocarbodiimidazole can then be added to (2) to give the N1-(isothiocyanato-phenyl)-)-N1,N2,N2-trimethylethane-1,2-diamine (3).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835464B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-3d3d43bde741434782933f206dc1ee08 |
| 출처 메모 | uspto-grants-2014_09 |