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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 76091생성일: 2026년 10월 25일

1,2-Ethanediamine, N1,N1,N2-trimethyl- → Bis-benzyloxy benzoic acid

https://huagongshe.com/reaction/76091

반응식

참여 물질

역할이름HCID투입량
반응물1,2-Ethanediamine, N1,N1,N2-trimethyl-HCID 67338—
반응물Methyl 2,3-bis(benzyloxy)benzoateHCID 10665397—
생성물Bis-benzyloxy benzoic acidHCID 10520703—

반응 단계

In another embodiment the compounds can be prepared as shown in Scheme IV. A bromo-nitrobenzene (1) can be reacted with N1,N2,N2-trimethylethane-1,2-diamine to give N1-(nitrophenyl)-N1,N2, N2-trimethylethane-1,2-diamine (2). A solution of (2) in can be subjected to hydrogenation, passed through a short pad of celite, washed with MeOH and evaporated under reduced pressure. Thiocarbodiimidazole can then be added to (2) to give the N1-(isothiocyanato-phenyl)-)-N1,N2,N2-trimethylethane-1,2-diamine (3).

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08835464B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-3d3d43bde741434782933f206dc1ee08
출처 메모uspto-grants-2014_09