Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 2-Oxopyrrolidine-3-carboxylic acid
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | Sodium Hydroxide | HCID 14798 | — |
| 반응물 | Ethyl 2-oxopyrrolidine-1-carboxylate | HCID 234959 | — |
| 생성물 | 2-Oxopyrrolidine-3-carboxylic acid | HCID 13474370 | — |
반응 단계
To 0.50 g (3.18 mmol) 2-oxo-pyrollidine-carboxylic acid ethyl ester in 10 mL EtOH are added 5 mL aq. NaOH (1M) solution. The reaction mixture is stirred at r.t. for 3 h. The EtOH is removed in vacuo and the residue is diluted with water and acidified with aq. HCl (2M) solution. The resulting precipitate is filtered and dried.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835472B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-eb7275050f334e848da4cf494465570b |
| 출처 메모 | uspto-grants-2014_09 |