Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
3-Oxocyclopentanecarboxylic acid → HCID 178441291, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 3-Oxocyclopentanecarboxylic acid | HCID 227798 | — |
| 반응물 | 2-tert-Butyl-4-butylisothiazol-5(2H)-imine | HCID 66867228 | — |
| 생성물 | HCID 178441291 | HCID 178441291 | — |
반응 단계
The product from Example 92B and 3-oxocyclopentanecarboxylic acid (Aldrich) were processed using the method described in Example 92C to afford the title compound. 1H NMR (DMSO-d6) δ 0.91 (t, J=7.5 Hz, 3H), 1.25-1.36 (m, 2H), 1.57 (s, 9H), 1.55-1.84 (m, 2H), 1.98-2.06 (m, 1H), 2.13-2.28 (m, 3H), 2.39-2.42 (m, 2H), 2.61-2.66 (m, 2H), 3.27-3.34 (m, 1H), 8.55 (s, 1H). MS (ESI+) m/z 323 (M+H)+. Anal. calcd. for C17H26N2O2S: C, 63.32; H, 8.13; N, 8.69. Found: C, 63.19; H, 8.07; N, 8.66.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08835475B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-6187a47ae84340b19d3a641f0e5b7e4c |
| 출처 메모 | uspto-grants-2014_09 |