참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Acetic Acid | HCID 176 | — |
| 반응물 | Nitromethane | HCID 6375 | — |
| 반응물 | Ammonium Acetate | HCID 517165 | — |
| 반응물 | 4-(5-Methyl-pyridin-2-yloxymethyl)-benzaldehyde | HCID 59255142 | — |
| 용매 | Water | HCID 962 | — |
| 용매 | Ethyl Acetate | HCID 8857 | — |
| 생성물 | HCID 59255428 | HCID 59255428 | 100.4% |
반응 단계
To an acetic acid (20.0 mL) solution of 4-(5-methyl-pyridin-2-yloxymethyl)-benzaldehyde (2.93 g, 12.9 mmol) described in Manufacturing Example 44-1-2 were added nitromethane (3.94 g, 64.5 mmol) and ammonium acetate (1.99 g, 25.8 mmol) under nitrogen atmosphere at room temperature, which was stirred for 2.5 hours at 100° C. Water and ethyl acetate were added to the reaction mixture, and the organic layer was extracted with ethyl acetate. This organic layer was washed with water and saturated aqueous sodium chloride, dried over anhydrous magnesium sulfate, and filtered. The filtrate was concentrated under a reduced pressure to obtain the title compound (3.50 g) as a crude product.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
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| 특허 번호 | US08841327B2 |
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| 출처 데이터셋 | uspto-grants-2014_09 |
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| ORD ID | ord-e6256274e4a94f8cafdaaaa5fc21d1c1 |
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| 출처 메모 | uspto-grants-2014_09 |
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