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Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
HRID 78239생성일: 2026년 10월 25일

(4-Phenylsulfanylmethyl-phenyl)-methanol → 4-[(Phenylsulfanyl)methyl]benzaldehyde

https://huagongshe.com/reaction/78239

반응식

참여 물질

역할이름HCID투입량
반응물(4-Phenylsulfanylmethyl-phenyl)-methanolHCID 59255239—
촉매HCID 178418406HCID 178418406—
용매ChloroformHCID 6212—
생성물4-[(Phenylsulfanyl)methyl]benzaldehydeHCID 82024199.9%

반응 단계

To a chloroform (10 mL) solution of (4-phenylsulfanylmethyl-phenyl)-methanol (1 g, 4.34 mmol) described in Manufacturing Example 206-1-2 was added manganese dioxide (3.77 g, 43.4 mmol), which was stirred for 15 hours at room temperature. The manganese dioxide was removed with a Celite bed, and the filtrate was concentrated under a reduced pressure to obtain the title compound (990 mg). The title compound was used in the following reaction without any further purification.

출처 및 근거

DOI10.6084/m9.figshare.5104873.v1
특허 번호US08841327B2
출처 데이터셋uspto-grants-2014_09
ORD IDord-d2e1aca90f0b464ba40b7ec81c7bcbb3
출처 메모uspto-grants-2014_09