Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Furan, 2-(bromomethyl)tetrahydro- → 4,5-Dimethyl-3-(tetrahydrofuran-2-ylmethyl)-1,3-thiazol-2(3H)-ylideneamine hydrobromide
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Furan, 2-(bromomethyl)tetrahydro- | HCID 14501 | — |
| 반응물 | 2-Amino-4,5-dimethyl-1,3-thiazole | HCID 73238 | — |
| 생성물 | 4,5-Dimethyl-3-(tetrahydrofuran-2-ylmethyl)-1,3-thiazol-2(3H)-ylideneamine hydrobromide | HCID 68621760 | — |
반응 단계
A mixture of 2-amino-4,5-dimethylthiazole and 2-(bromomethyl)tetrahydrofuran were processed using the method described in Example 12A to afford the title compound. 1H NMR (300 MHz, DMSO-d6) δ ppm 1.43-1.64 (m, 1H) 1.73-2.00 (m, 3H) 2.17 (s, 3H) 2.19 (s, 3H) 3.53-3.68 (m, 1H) 3.71-3.85 (m, 1H) 3.91-4.17 (m, 3H) 9.34 (s, 1H),), MS (DCI/NH3) m/z 212 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08841334B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-fe8c0ca38329459780cca436ad88484e |
| 출처 메모 | uspto-grants-2014_09 |