참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Chlorocyclopentanone | HCID 12751 | — |
| 반응물 | Thiourea | HCID 2723790 | — |
| 생성물 | 3,4,5,6-Tetrahydro-2H-cyclopenta(d)(1,3)thiazol-2-imine | HCID 332255 | — |
반응 단계
A mixture of 2-chlorocyclopentanone (5.0 g, 40 mmol) and thiourea (3.0 g, 40 mmol) was heated at 70° C. for 3 hours. After cooling, the solid was triturated with ethanol and collected by filtration to afford the title compound. MS (ESI) m/z 141 (M+H)+.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08841334B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-d641966f5d9548f29add4af141aa5c0f |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
