Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Methanol → HCID 59471788, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Methanol | HCID 887 | — |
| 반응물 | Sulfuric Acid | HCID 1118 | — |
| 반응물 | 3-Amino-6-(pyridin-3-yl)pyrazine-2-carboxylic acid | HCID 59472154 | — |
| 생성물 | HCID 59471788 | HCID 59471788 | 97% |
반응 단계
To 3-amino-6-(3-pyridyl)pyrazine-2-carboxylic acid (2 g, 9.251 mmol) in MeOH (50 mL) was added conc. H2SO4 (907.3 mg, 493.1 μL, 9.251 mmol) and the mixture heated to reflux for 2 hours. The solvent was removed in vacuo and the mixture neutralised with aq. Na2CO3. The resulting brown solid was collected by filtration and dried (2.08 g, 97% Yield). MS (ES+) 231
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08841308B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-8282d7038caf4e1194a7dd66edba6051 |
| 출처 메모 | uspto-grants-2014_09 |