Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Phosgen toluene → HCID 86709886, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Phosgen toluene | HCID 19083224 | — |
| 반응물 | 4-(2-(2-(2-Methoxyethoxy)ethoxy)ethoxy)aniline | HCID 21917640 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 86709886 | HCID 86709886 | — |
반응 단계
To a stirred 0° C. solution of 18 (0.59 g, 2.29 mmol) in DCM (23 mL) was added a 20% phosgene/toluene solution (2.42 mL). After stirring for 3 h the reaction mixture was concentrated under reduced pressure and carried on without further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08841460B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-4d9ae502f1a9421a908e220b967daec3 |
| 출처 메모 | uspto-grants-2014_09 |