Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 6-Methoxy-1-propyl-indan
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 5-methoxy-1-propyl-1H-indene | HCID 21990907 | — |
| 촉매 | Palladium | HCID 23938 | — |
| 생성물 | 6-Methoxy-1-propyl-indan | HCID 21990933 | — |
반응 단계
The mixture of indenes from step 1 (1.24 g, approx. 6.1 mmol) was dissolved in ethanol (40 mL), treated with 10% Pd on carbon (58 mg), and hydrogenated at 40 psi and room temperature for 60 minutes. The catalyst was removed by filtration and the filtrate was evaporated under vacuum to provide a mixture (1.287 g) of 6-methoxy-1-propyl-indan and 5-methoxy-1-propyl-indan in nearly a 1:1 ratio.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087599B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-f7b0953821a446b293b603d05a892eeb |
| 출처 메모 | uspto-grants-2006_08 |