참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Potassium Carbonate | HCID 11430 | — |
| 반응물 | (3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-yl acetate | HCID 59959307 | — |
| 용매 | Methanol | HCID 887 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | (3R,3aS,6aR)-hexahydrofuro(2,3-b)furan-3-ol | HCID 9942150 | — |
반응 단계
(3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-yl acetate (8.0 g) was dissolved in dichloromethane (24 ml) and Methanol (24 ml). Potassium carbonate (0.1 g) was added and reaction mass was stirred at 25-35° C. till the completion of reaction. Reaction mass was filtered & concentrated under vacuum at 40-45° C. to residue of (3R,3aS,6aR)-Hexahydrofuro[2,3-b]furan-3-ol (Yield 6.5 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08841467B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-7fb413531e564110ada8de0058b82c76 |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
