Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Thionyl Chloride → HCID 66937557, 화합물
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Thionyl Chloride | HCID 24386 | — |
| 반응물 | (1,5-Dimethyl-1H-Pyrazol-3-Yl)Methanol | HCID 2776366 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | HCID 66937557 | HCID 66937557 | 101.8% |
반응 단계
To (1,5-dimethyl-1H-pyrazol-3-yl)methanol (5.01 g, 39.71 mmol) in DCM (80 mL) at 0° C. was cautiously added thionyl chloride (25 mL, 343.6 mmol). The cold bath was removed and the reaction mixture was stirred at ambient temperature for 3 hours. The reaction mixture was concentrated under reduced pressure to give crude product (7.32 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08841455B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-a0e28097d0434a88bd9c842f43cfe4a0 |
| 출처 메모 | uspto-grants-2014_09 |