Chloroacetyl chloride → HCID 178448915, 화합물

HRID 80018

반응식

HRID 80018 반응식
[CH3:1][C:2]1[CH:3]=[CH:4][CH:5]=[CH:6][C:7]=1[NH2:8].Cl[CH2:10][C:11](Cl)=[O:12].[CH2:14]([N:18]=[C:19]=[S:20])[CH2:15][CH2:16][CH3:17]>>[CH2:14](/[N:18]=[C:19]1\[S:20][CH2:10][C:11](=[O:12])[N:8]\1[C:7]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[CH3:1])[CH2:15][CH2:16][CH3:17]

참가 물질

4

반응물 3

HCID 6577Chloroacetyl chlorideHCID 7242O-ToluidineHCID 11613Butyl Isothiocyanate

생성물 1

HCID 178448915HCID 178448915, 화합물

실험 절차

2-[(Z)-n-butylimino]-3-(2-methylphenyl)-thiazolidin-4-one is prepared following Method B and starting from o-tolylamine, chloroacetyl chloride and n-butylisothiocyanate. LC-MS: tR=0.77 min, [M+1]+=263, 1H NMR (CDCl3): δ 7.35-7.28 (m, 3H), 7.14-7.10 (m, 1H), 4.01 (s, 2H), 3.38-3.22 (, 2H), 2.18 (s, 3H), 1.59-1.47 (m, 2H), 1.38-1.25 (m, 2H), 0.90 (t, J=7.0 Hz, 3H).

출처 및 근거

ORD 기록
ord-5521928cb4834d1498a8d78df5a60127
출처 데이터셋
uspto-grants-2014_09
특허 번호
USRE045174E1

연결된 노트

불러오는 중…