Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Water → 2-((Triphenylmethyl)amino)ethanol
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Water | HCID 962 | — |
| 반응물 | Trityl chloride | HCID 6456 | — |
| 반응물 | Acetaldehyde ammonia | HCID 522583 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | 2-((Triphenylmethyl)amino)ethanol | HCID 3125608 | 39% |
반응 단계
Triphenylchloromethane (1.00 g, 3.58 mmol) (Wako Pure Chemical Industries, Ltd.) and aminoethanol (2.00 g, 32.7 mmol) were dissolved in acetonitrile (5 mL), and the solution was stirred at room temperature overnight. Water (100 mL) was poured into the reaction solution, and the precipitates were suction-filtered and then dried. The solid product was recrystallized from a mixed solvent of ethanol (Wako Pure Chemical Industries, Ltd.) and water, to thereby obtain the title compound (0.43 g, 39% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846012B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-c8024df5c705406a8ff8676a83e574f1 |
| 출처 메모 | uspto-grants-2014_09 |