Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Iodoethane → Ethyl(triphenylmethyl)amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Iodoethane | HCID 6340 | — |
| 반응물 | Tritylamine | HCID 138598 | — |
| 용매 | Acetonitrile | HCID 6342 | — |
| 생성물 | Ethyl(triphenylmethyl)amine | HCID 4447360 | 28% |
반응 단계
Triphenylmethylamine (1.00 g, 3.86 mmol) (Wako Pure Chemical Industries, Ltd.) and iodoethane (1.50 g, 9.62 mmol) (Wako Pure Chemical Industries, Ltd.) were dissolved in acetonitrile (5 mL) (Wako Pure Chemical Industries, Ltd.), and the mixture was left to stand still at room temperature for 3 days. The solvent was distilled off under reduced pressure, and the residue was subjected to silica gel column chromatography (chloroform (Wako Pure Chemical Industries, Ltd.) as an eluent), to thereby obtain the title compound (0.31 g, 28% yield).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846012B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-b13daa3783284fc5acaee76552dcdb91 |
| 출처 메모 | uspto-grants-2014_09 |