2-Chlorobenzylamine → HCID 66988151, 화합물

반응식

[Na].O[CH:3]=[C:4]1[CH2:8][CH2:7][O:6][C:5]1=[O:9].[Cl:10][C:11]1[CH:18]=[CH:17][CH:16]=[CH:15][C:12]=1[CH2:13][NH2:14]>>[Cl:10][C:11]1[CH:18]=[CH:17][CH:16]=[CH:15][C:12]=1[CH2:13][NH:14][CH:3]=[C:4]1[CH2:8][CH2:7][O:6][C:5]1=[O:9]

참가 물질

반응물 2

HCID 666482-Chlorobenzylamine

HCID 66988753HCID 66988753, 화합물

생성물 1

HCID 66988151HCID 66988151, 화합물수율 75%

실험 절차

Using 3-hydroxymethylenedihydrofuran-2-one sodium salt (10 mmol) and 2-chlorobenzylamine (11 mmol) and proceeding according to the abovementioned method A2, 3-(2-chlorobenzylamino)methylenedihydrofuran-2-one (1.54 g, efficiency: 75%) is produced in the form of a white powder.

출처 및 근거

ORD 기록: ord-7bafc3a5c1d741cc8d041f507b2fad31
출처 데이터셋: uspto-grants-2014_09
DOI: 10.6084/m9.figshare.5104873.v1
특허 번호: US08846125B2

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