Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Triethylamine → N-[(4-chlorophenyl)methyl]-N',N'-diethylethane-1,2-diamine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Triethylamine | HCID 8471 | — |
| 반응물 | 4-Chlorobenzylamine | HCID 66036 | — |
| 반응물 | 2-Bromoethyldiethylammonium bromide | HCID 70607 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | N-[(4-chlorophenyl)methyl]-N',N'-diethylethane-1,2-diamine | HCID 296048 | — |
반응 단계
4-Chlorobenzylamine (1.0 mL, 8.2 mmol) was added to a solution of 2-bromo-N,N-diethylethylamine hydrobromide (2.4 g, 9.0 mmol) and triethylamine (3.4 mL, 25 mmol) in dichloromethane (16 mL). The mixture was stirred at room temperature for 5 hours. The mixture was then concentrated to give N1-(4-chlorobenzyl)-N2,N2-diethylethane-1,2-diamine as an oil which was used immediately without purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US08846683B2 |
| 출처 데이터셋 | uspto-grants-2014_09 |
| ORD ID | ord-ea6cfcefd4a7480d8470f1ed94ea21d7 |
| 출처 메모 | uspto-grants-2014_09 |