Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrogen Peroxide → Peroxide, bis(2-methyl-1-oxopropyl)
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrogen Peroxide | HCID 784 | — |
| 반응물 | Isobutyryl chloride | HCID 62325 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | Peroxide, bis(2-methyl-1-oxopropyl) | HCID 76969 | — |
반응 단계
In Example A, the procedure of WO 01/32613 was repeated. First, a solution of Na2O2 was prepared by combining 108.3 g of demineralized water, 18.5 g of NaOH-33 solution, and 3.7 g of the aqueous H2O2. A second reactor was charged with 33.3 g of demineralized water, 27.7 g of the PVA solution, and 16.3 g of isobutanoyl chloride while controlling the temperature between 5–10° C. Next, the Na2O2 solution was dosed while the system was homogenized. No diisobutanoyl peroxide was obtained and only an aqueous phase formed.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087693B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-9ab80e1ebfc347c382d0c4a31e189f35 |
| 출처 메모 | uspto-grants-2006_08 |