4-Acetoxy-3-phenyl-but-2-enoic acid methyl ester → 4-Acetoxy-3-phenyl-butyric Acid Methyl Ester
반응식
[CH3:1][O:2][C:3](=[O:17])[CH:4]=[C:5]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[CH2:6][O:7][C:8](=[O:10])[CH3:9]>[Pd].C(O)(=O)C>[CH3:1][O:2][C:3](=[O:17])[CH2:4][CH:5]([C:11]1[CH:16]=[CH:15][CH:14]=[CH:13][CH:12]=1)[CH2:6][O:7][C:8](=[O:10])[CH3:9]참가 물질
4
실험 절차
A mixture of 4-acetoxy-3-phenyl-but-2-enoic acid methyl ester, (1.0 g, 4.27 mmol), 10 wt. % palladium on activated carbon (1.0 g), acetic acid (10 mL) is shaken under an atmosphere of hydrogen on a Parr® Shaker. The mixture is filtered through a pad of Celite® and rinsed with methanol. The solution is concentrated in vacuo to yield 0.93 g (92%) of the title compound.
후처리
- filtrationThe mixture is filtered through a pad of Celite®
- washrinsed with methanol
- concentrationThe solution is concentrated in vacuo
출처 및 근거
- ORD 기록
- ord-2d0268180b8e432b931028249aef5399
- 출처 데이터셋
- uspto-grants-2006_08
- 특허 번호
- US07087626B2
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