참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Trifluoroacetic acid | HCID 6422 | — |
| 반응물 | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester | HCID 69920127 | — |
| 용매 | Dichloromethane | HCID 6344 | — |
| 생성물 | Amino-acetic acid 4-allyl-2-methoxy-phenyl ester Trifluoroacetate | HCID 86674925 | — |
반응 단계
To a solution of compound amino-acetic acid 4-allyl-2-methoxy-phenyl ester (0.3 g) in DCM (10 mL) was added trifluoroacetic acid (0.5 mL) drop wise at (0° C.). The mixture was allowed to stir at room temperature (25° C.) over a period of 2 h. Solvent was stripped off completely and the reaction was carried for the next step (510 mg).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08846721B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-94416477fee4402b9dae8b9b83cdb00f |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
