참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | Carbon Disulfide | HCID 6348 | — |
| 반응물 | 2,3-Diaminopyridine | HCID 9956 | — |
| 용매 | Ethanol | HCID 702 | — |
| 생성물 | HCID 178527819 | HCID 178527819 | — |
반응 단계
To a solution of pyridine-2,3-diamine (5 g) in EtOH (150 ml) was added carbon disulfide (23 mL) at room temperature. The mixture was stirred at 40° C. under Ar for 10 h. The mixture was cooled to room temperature. The resulting white solid was filtered and washed with ether to give 1H-imidazo[4,5-b]pyridine-2-thiol (5.61 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US08846713B2 |
|---|
| 출처 데이터셋 | uspto-grants-2014_09 |
|---|
| ORD ID | ord-ea7d4add4185470b924efe62d498fe9b |
|---|
| 출처 메모 | uspto-grants-2014_09 |
|---|
