Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Ethanol → 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Ethanol | HCID 702 | — |
| 반응물 | 2-Bromo-1-(4-hydroxyphenyl)ethanone | HCID 4964 | — |
| 반응물 | HCID 66824522 | HCID 66824522 | — |
| 생성물 | 2-[4-Hydroxyphenyl]-8-methylimidazo[1,2-a]pyridine | HCID 22015659 | — |
반응 단계
The product of step A (30 g) and 2-aminopicoline (15 mL) in ethanol (200 mL) was heated at reflux temperature for 4 hours then cooled to ambient temperature. The resulting precipitate containing the title compound was isolated via filtration (27 g).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US07087757B2 |
| 출처 데이터셋 | uspto-grants-2006_08 |
| ORD ID | ord-b69a26f17c554d17b35eebf5deba32e4 |
| 출처 메모 | uspto-grants-2006_08 |