Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
2,4,5-Trichloroaniline → (Methylsulfonyl)(2,4,5-trichlorophenyl)amine
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | 2,4,5-Trichloroaniline | HCID 12487 | — |
| 반응물 | Methanesulfonyl chloride | HCID 31297 | — |
| 용매 | O-Xylene | HCID 7237 | — |
| 생성물 | (Methylsulfonyl)(2,4,5-trichlorophenyl)amine | HCID 2427123 | — |
반응 단계
A mixture of 2,4,5-trichloroaniline (39.3 g.), methane sulfonyl chloride (22.9 g.) and 100 ml. of xylene were heated together under reflux conditions for 18 hours. The mixture was then allowed to cool, which formed a brown precipitate. The product was worked up in the same manner as set forth in Example 1 to yield 24.0 g. of product, m.p. 144°-145° C.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04093445 |
| 출처 데이터셋 | uspto-grants-1978_06 |
| ORD ID | ord-821e4309e95646ffa6a425d6d741ea1e |
| 출처 메모 | uspto-grants-1978_06 |