Tert-Butylamine → HCID 20325511, 화합물

HRID 838980노트

반응식

HRID 838980 반응식
[O:1]1[CH2:16][CH:2]1[CH2:3][O:4][C:5]1[CH:14]=[C:13]2[C:8]([CH:9]=[N:10][NH:11][C:12]2=[O:15])=[CH:7][CH:6]=1.[C:17]([NH2:21])([CH3:20])([CH3:19])[CH3:18]>>[C:17]([NH:21][CH2:16][CH:2]([OH:1])[CH2:3][O:4][C:5]1[CH:14]=[C:13]2[C:8]([CH:9]=[N:10][NH:11][C:12]2=[O:15])=[CH:7][CH:6]=1)([CH3:20])([CH3:19])[CH3:18]

참가 물질

3

반응물 2

HCID 6385Tert-ButylamineHCID 203254967-(2,3-Epoxypropoxy)-1(2H)-phthalazinone

생성물 1

HCID 20325511HCID 20325511, 화합물

실험 절차

7-(2,3-Epoxypropoxy)-1(2H)-phthalazinone was reacted with t-butylamine in a similar manner to that described in Example 1(iv) to give 7-(3-t-butylamino-2-hydroxypropoxy)-1(2H)-phthalazinone, the hydrochloride of which was recrystallised from ethanol and had m.p. 263°-264° (decomp).

출처 및 근거

ORD 기록
ord-f7460ea83b9a407584fabeec8bf63be9
출처 데이터셋
uspto-grants-1978_06
특허 번호
US04093725

반응 노트

불러오는 중…