Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
p-Toluenesulfonyl isocyanate → 5-PHENYL-2-[N-p-TOLUENESULFONYLCARBAMOYL]-1,3-CYCLOHEXANEDIONE
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | p-Toluenesulfonyl isocyanate | HCID 77703 | — |
| 반응물 | 1,3-Cyclohexanedione, 5-phenyl- | HCID 568962 | — |
| 용매 | Benzene | HCID 241 | — |
| 생성물 | 5-PHENYL-2-[N-p-TOLUENESULFONYLCARBAMOYL]-1,3-CYCLOHEXANEDIONE | HCID 20325601 | — |
반응 단계
Reaction of equimolar amounts of 5-phenyl-1,3-cyclohexanedione with p-toluenesulfonylisocyanate in benzene according to the procedure of Example 1 affords 5-PHENYL-2-[N-p-TOLUENESULFONYLCARBAMOYL]-1,3-CYCLOHEXANEDIONE, m.p. 163.5°-166° C. (corr.).
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04093741 |
| 출처 데이터셋 | uspto-grants-1978_06 |
| ORD ID | ord-922e8597dd3447b3b7aa65738553df05 |
| 출처 메모 | uspto-grants-1978_06 |