Huagongshe화공사 화학 정보 인쇄 보고서 · 연구 참고용
Hydrochloric Acid → 1-(1-Chloroethyl)-3-methoxybenzene
참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|---|---|---|
| 반응물 | Hydrochloric Acid | HCID 313 | — |
| 반응물 | (+-)-1-(3-Methoxyphenyl)ethanol | HCID 90902 | — |
| 용매 | Water | HCID 962 | — |
| 생성물 | 1-(1-Chloroethyl)-3-methoxybenzene | HCID 12861413 | — |
반응 단계
Into a solution of 152.1 g (1 mol) of 1-(3'-methoxyphenyl)-ethan-1-ol in 750 ml petroleum ether, one introduces hydrogen chloride during ice cooling until water separation is completed. The organic phase is then washed with ice-cold water, dried and the petroleum ether is removed in vacuo. The thermo-labile residue is used without any further purification.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| 특허 번호 | US04094994 |
| 출처 데이터셋 | uspto-grants-1978_06 |
| ORD ID | ord-741b9bf5f4a34758aa2a5e85ba27fdb7 |
| 출처 메모 | uspto-grants-1978_06 |