참여 물질
| 역할 | 이름 | HCID | 투입량 |
|---|
| 반응물 | 2-Naphthol | HCID 8663 | — |
| 반응물 | Methylcarbamoyl chloride | HCID 80931 | — |
| 용매 | Cumene | HCID 7406 | — |
| 생성물 | beta-Carbaryl | HCID 77710 | 85% |
반응 단계
72 parts by weight of β-naphthol are dissolved in 250 parts by weight of cumene at 80° C. 46.7 parts by weight of methylcarbamyl chloride are stirred into this solution over a period of 10 minutes while nitrogen is simultaneously bubbled through the solution. The reaction is complete after 15 minutes. The hot reaction solution is cooled to 0° C and the precipitated β-naphthyl-N-methylcarbamate is isolated. The yield is 85% of theory.
출처 및 근거
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| 특허 번호 | US04095034 |
|---|
| 출처 데이터셋 | uspto-grants-1978_06 |
|---|
| ORD ID | ord-48170774383b4672ab738f47bfbf4459 |
|---|
| 출처 메모 | uspto-grants-1978_06 |
|---|
